ELECTRON
CRYSTALLOGRAPHY
A deep dive into nanocrystals
AIC2023 International School
Timetable
3rd July (Day 1)
8.00 -9.00 Registration 9.00 -10.45 Crystallography and diffraction: Introduction to crystallography, a crystal in real and reciprocal space, the diffraction as a tool, with a direct reference always to electrons Enrico Mugnaioli 10.45-11.00 Coffee break 11.00-11.45 The TEM as a diffractometer: Introduction to the TEM instrument, electron optics, imaging and diffraction, how a TEM works Mauro Gemmi 11.45-12.30 Diffraction from accelerated electrons: geometry of electron diffraction, SAED, NED, precession electron diffraction and 3D ED as final goalEnrico Mugnaioli 12.30-14.00 Lunch 14.00-15.45 3D ED data collection: different possible data collections type with ED Mauro Gemmi 15.45-16.00 Coffee break 16.00-17.30 3D ED data reduction and analysisPetr Brazda
4th July (Day 2)
9.00-10.45 Structure solution with 3D ED dataBenedetta Carrozzini 10.45-11.00 Coffee break 11.00-12.45 Kinematical structural refinement with 3D ED data: how to refine a crystal structure kinematicallyTim Gruene 12.45-14.00 Lunch 14.00-17.30 Practicals
Group 1 Kinematical refinement with SHELX Tim Gruene, Faye, Daniele Marchetti Structure solution with SIR Benedetta Carrozzini, Mauro Gemmi Data analysis with PETS2 Petr Brazda, Faye, Daniele Marchetti
Group 2 Structure solution with SIR Benedetta Carrozzini, Mauro Gemmi Data analysis with PETS2 Petr Brazda, Faye, Daniele Marchetti Kinematical refinement with SHELX Tim Gruene, Faye, Daniele Marchetti
Group 1 Kinematical refinement with SHELX Tim Gruene, Faye, Daniele Marchetti Structure solution with SIR Benedetta Carrozzini, Mauro Gemmi Data analysis with PETS2 Petr Brazda, Faye, Daniele Marchetti
Group 2 Structure solution with SIR Benedetta Carrozzini, Mauro Gemmi Data analysis with PETS2 Petr Brazda, Faye, Daniele Marchetti Kinematical refinement with SHELX Tim Gruene, Faye, Daniele Marchetti
5th July (Day 3)
9.00-9.45 Dynamical refinementPetr Brazda 9.45-10.30 Structure analysis of inorganic compoundsMauro Gemmi, Enrico Mugnaioli 10.30-10.45 Coffee break 10.45-11.30 Structure analysis of organic compoundsTatiana Gorelik 11.30-12.15 Challenging problems and 3D ED data: small molecules, H determination, absolute structure Petr Brazda 12.15-14.00 Lunch 14.00-17.30 Practicals Data analysis with PETS2 Petr Brazda, Faye, Daniele Marchetti Kinematical refinement with SHELX Tim Gruene, Faye, Daniele Marchetti Structure solution with SIR Benedetta Carrozzini, Mauro Gemmi Instrument tour Enrico Mugnaioli, Paoli, Michele Alderighi Dynamical refinement with JANA Petr Brazda, Mauro Gemmi
6th July (Day 4)
9.00-10.45 3D ED for macromoleculesGerhard Hofer 10.45-11.00 Coffee break 11.00- 11.45 Texture and phase analysis: (ASTAR), 4D STEMMuriel Veron 11.45-12.30 Disorder quantification and 2D crystalsTatiana Gorelik 12.30-14.00 Lunch 14.00-16.00 Practicals Dynamical refinement with JANA Petr Brazda, Mauro Gemmi Instrument tour Enrico Mugnaioli, Paoli, Michele Alderighi 16.00-17.00 Final round table
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